Biomolecular NMR Facility

Department of Chemistry and Biochemistry

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NMR Spectrometers 800MHz NMR Installation
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C13_DEPT 2D for Structure Analysis Saturation Transfer Differenace (STD) Diffusion Ordered Spectroscopy(DOSY) RNA HSQC Protein Sequential Assignment Protein NOESY NMR Titration Parallel Stranded DNA Probe Sensitivity
NMR Sample Preparation Experiment Preparation 1D 1H 1D 31P 1D WaterGate 2D Experiment Setup 1H-15N HSQC 1H-13C HSQC 1H-15N SoFast-HMQC 2D TOCSY 2D NOESY Triple Resonance Experiments Saturation Transfer Difference NMR BBFO Probe Experiments Non-Uniform Sampling(NUS)
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  CP600 NMR600 CP800
Magnet Ultrashield 600 MHz Ultrashield Plus 600 MHz Ascend 800 MHz
Console Avance III Avance III Avance III HD
Probe

CP2.1 TCI H&F CryoProbe (QCI-F)

CPTXI 600S3 H-C/N-D-05 Z Cryoprobe

BBO 600S3 BBF-H-D-05 Z SP

TXI 600SB H-C/N-D-05 Z BTO

CPQCI 1H-31P/13C/15N/D Z-GRD Cryoprobe

PATXI 800S4 H-C/N-D-05 Z

Sensitivity

CPQCI: 1H 6000:1; 19F 5000:1

CPTXI: 1H 4000:1; 13C 170:1

 TXI: 1H 1000:1

CPQCI: 1H 7000:1; 13C 1400:1; 31 P 250:1

PATXI: 1H 2000:1

Sample Temperature 5-35°C 5-60°C 5-105 °C
Software TopSpin3.7 TopSpin3.7 TopSpin3.7
Features
  • High sensitivity
  • High resolution
  • Triple resonance capability
  • Sufficient for high resolution routine 1D, 2D and 3D experiments
  • High throughput ready
  • Triple resonance capability
  • Broadband nuclei measurements
  • High sensitivity
  • High resolution
  • 13C, 31P direct detection
  • High temperature sample analysis
  • Quadruple capability
  • Automatic tune and shim

spectrometers

Bruker 800 MHz NMR Installation